_diffrn.id 'Set1'
_diffrn.ambient_temp 293(3)
_diffrn.ambient_environment
; Mother liquor from the reservoir of the vapor diffusion experiment,
mounted in room air
;
_diffrn.crystal_support
; 0.7 mm glass capillary, sealed with dental wax
;
_diffrn.crystal_treatment
; Equilibrated in rotating anode radiation enclosure for 18 hours prior
to beginning of data collection.
;
_diffrn.id 'd1'
_diffrn.details
;
\q scan width (1.0 + 0.14tan\q)\%, \q scan rate 1.2\% per min.
Background counts for 5 sec on each side every scan.
;
_diffrn.ambient_temp 293
_diffrn.id 1
_diffrn.ambient_temp 298